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However, I now believe that only a 4x mol. eq. is required for the first part, or 150 g, then maybe add 50 g before the copper. This is after finding other reports. Add the first half of the boro when the temps have dropped (won't react with water as much at lower temps) making sure it is finely crushed before pouring in. 4) Calculate CuCl:-2H2O amount.